HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2079496Erstellt: 26. Oktober 2026
Potassium Carbonate → 4-tert-Butyl-N-[4-chloro-2-(methoxy-pyridin-4-yl-methyl)-Phenyl]-benzenesulfonamide
https://huagongshe.com/reaction/2079496
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 4-tert-Butyl-N-[4-chloro-2-(chloro-pyridin-4-yl-methyl)-phenyl]-benzenesulfonamide | HCID 59485502 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 4-tert-Butyl-N-[4-chloro-2-(methoxy-pyridin-4-yl-methyl)-Phenyl]-benzenesulfonamide | HCID 59756865 | — |
Reaktionsschritte
A suspension of 4-tert-butyl-N-[4-chloro-2-(chloro-pyridin-4-yl-methyl)-phenyl]-benzenesulfonamide (113 mg, 0.25 mmol) and potassium carbonate (69 mg, 0.5 mmol) in anhydrous methanol was heated at 60° C. overnight, the solid residue was then removed by filtration and product was purified by preparative HPLC. MS: (M+H)=445.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US07932252B2 |
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| Quelldatensatz | uspto-grants-2011_04 |
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| ORD ID | ord-8243154651194dda942bd5f33ca62a72 |
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| Quellennotiz | uspto-grants-2011_04 |
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