HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(5-Oxiranyl-furan-2-yl)-[1,3]dioxolane → (5-[1,3]Dioxolan-2-yl-furan-2-yl)-acetaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(5-Oxiranyl-furan-2-yl)-[1,3]dioxolane | HCID 23130765 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | (5-[1,3]Dioxolan-2-yl-furan-2-yl)-acetaldehyde | HCID 86042298 | 69,8% |
Reaktionsschritte
The resulting 2-(5-oxiranyl-furan-2-yl)-[1,3]dioxolane (2.25 g) and silica gel (5.00 g) were suspended in ethyl acetate (40 mL), and the solution was stirred for 6.5 hours at room temperature. The reaction solution was filtered, then, the filtrate was evaporated in vacuo, and (5-[1,3]dioxolan-2-yl-furan-2-yl)-acetaldehyde (1.57 g) was obtained as a yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07932272B2 |
| Quelldatensatz | uspto-grants-2011_04 |
| ORD ID | ord-e5c89323eebe410eaa5f3bbf613666b1 |
| Quellennotiz | uspto-grants-2011_04 |