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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2080137Erstellt: 25. Oktober 2026

3-(2-Methylpropenyl)-benzylamine → 3-Isobutylbenzylamine

https://huagongshe.com/reaction/2080137

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-(2-Methylpropenyl)-benzylamineHCID 23130720—
KatalysatorHCID 178418390HCID 178418390—
LösungsmittelEthanolHCID 702—
Produkt3-IsobutylbenzylamineHCID 2313055356,6%

Reaktionsschritte

3-(2-Methylpropenyl)-benzylamine described in Preparation Example 137 (100 mg, 0.621 mmol) was dissolved in ethanol (5 mL), 10% palladium-carbon (50% water wet, 20 mg) was added thereto, and the mixture was stirred for 2 hours at room temperature under hydrogen atmosphere. The catalyst was filtered, then, the solvent was evaporated, and the title compound (58 mg, 56.6%) was obtained as a colorless oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07932272B2
Quelldatensatzuspto-grants-2011_04
ORD IDord-f49fab2946984f2d92c5d12888688d44
Quellennotizuspto-grants-2011_04