HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(2-Methylpropenyl)-benzylamine → 3-Isobutylbenzylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(2-Methylpropenyl)-benzylamine | HCID 23130720 | — |
| Katalysator | HCID 178418390 | HCID 178418390 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-Isobutylbenzylamine | HCID 23130553 | 56,6% |
Reaktionsschritte
3-(2-Methylpropenyl)-benzylamine described in Preparation Example 137 (100 mg, 0.621 mmol) was dissolved in ethanol (5 mL), 10% palladium-carbon (50% water wet, 20 mg) was added thereto, and the mixture was stirred for 2 hours at room temperature under hydrogen atmosphere. The catalyst was filtered, then, the solvent was evaporated, and the title compound (58 mg, 56.6%) was obtained as a colorless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07932272B2 |
| Quelldatensatz | uspto-grants-2011_04 |
| ORD ID | ord-f49fab2946984f2d92c5d12888688d44 |
| Quellennotiz | uspto-grants-2011_04 |