Hydrazine → Tetradecanehydrazide

HRID 2081661

Reaktionsgleichung

Reaktionsgleichung von HRID 2081661
[NH2:1][NH2:2].[C:3]([O:18]C)(=O)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>CO>[C:3]([NH:1][NH2:2])(=[O:18])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 31284Methyl Myristate

Produkt 1

HCID 2748033TetradecanehydrazideAusbeute 43,9 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (1.9 mL, 0.058 mol) was added to a solution of methyl tetradecanoate (13.96 g, 0.058 mol) in methanol (300 mL) and the solution refluxed for 3 days. The mixture was allowed to cool and filtered to yield 6.17 g of a crystalline solid, m.p. 107°-111° C.

Aufarbeitung

  1. temperaturethe solution refluxed for 3 days
  2. temperatureto cool
  3. filtrationfiltered

Quellen und Nachweise

ORD-Eintrag
ord-afcf65b2ba08436fa2698374f5ed43d2
Quelldatensatz
uspto-grants-1993_02
Patentnummer
US05185358

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