HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethynylcyclohexane → 2-(3-Cyclopentyl-1-propyn-1-yl)adenosine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethynylcyclohexane | HCID 70263 | — |
| Edukt | 2-Iodoadenosine | HCID 169662 | — |
| Edukt | (Prop-2-yn-1-yl)cyclopentane | HCID 521007 | — |
| Produkt | 2-(3-Cyclopentyl-1-propyn-1-yl)adenosine | HCID 132348 | 70,3% |
Reaktionsschritte
The procedure of Example 1 was repeated except that 1.56 g (3.98 mmol) of 2-iodoadenosine was used as the starting compound and that the cyclohexylacetylene was replaced by 3-cyclopentylpropyne, whereby 1.05 g (2.8 mmol) of crystalline 2-(3-cyclopentyl-1-propynyl)adenosine was obtained (yield: 70.3%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05189027 |
| Quelldatensatz | uspto-grants-1993_02 |
| ORD ID | ord-c4dab15d462d4976a7538035653ba803 |
| Quellennotiz | uspto-grants-1993_02 |