3-Butylamino-4-phenoxy-5-sulphamyl-benzamide → (4-Benzyl-3-n-butoxy-5-sulfamylbenzyl)-2-diethylaminoethylamine
Reaktionsgleichung
C(NC1C=C(C=C(S(=O)(=O)N)C=1OC1C=CC=CC=1)C(N)=O)CCC.[CH2:26]([C:33]1[C:48]([S:49](=[O:52])(=[O:51])[NH2:50])=[CH:47][C:36]([C:37]([NH:39][CH2:40][CH2:41][N:42]([CH2:45][CH3:46])[CH2:43][CH3:44])=O)=[CH:35][C:34]=1[O:53][CH2:54][CH2:55][CH2:56][CH3:57])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[CH2:26]([C:33]1[C:48]([S:49](=[O:51])(=[O:52])[NH2:50])=[CH:47][C:36]([CH2:37][NH:39][CH2:40][CH2:41][N:42]([CH2:43][CH3:44])[CH2:45][CH3:46])=[CH:35][C:34]=1[O:53][CH2:54][CH2:55][CH2:56][CH3:57])[C:27]1[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=1Komponenten
3
Versuchsvorschrift
By replacing in Example 289 3-n-butylamino-4-phenoxy-5-sulfamylbenzamide with an equimolar amount of 4-benzyl-3-n-butoxy-5-sulfamyl-N-(2'-diethylaminoethyl)-benzamide and following the procedure described, (4-benzyl-3-n-butoxy-5-sulfamylbenzyl)-2-diethylaminoethylamine is obtained as a dihydrate with a melting point of 89°-93° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-c406f15c764b4a6b99b521c3d354eb75