HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,3-Dichlorothioanisole → 2',3'-Dichloro-4'-methylthio-2-cyclopentylacetophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,3-Dichlorothioanisole | HCID 2758224 | — |
| Edukt | Cyclopentylacetyl chloride | HCID 3485182 | — |
| Edukt | Aluminum(III) Chloride | HCID 6451240 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 2',3'-Dichloro-4'-methylthio-2-cyclopentylacetophenone | HCID 20358446 | — |
Reaktionsschritte
2', 3'-Dichloro-4'-methylthio-2-cyclopentylacetophenone is prepared following substantially the same procedure described in Example 10, Step A, using the following substances: 2,3-dichlorothioanisole (63.1 g., 0.327 mole), methylene chloride (300 ml.), cyclopentylacetyl chloride (52.7 g., 0.367 mole) and aluminum chloride (48.0 g., 0.36 mole).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04085219 |
| Quelldatensatz | uspto-grants-1978_04 |
| ORD ID | ord-be5d18dd93a745db843cdf455e658d4f |
| Quellennotiz | uspto-grants-1978_04 |