Chloroacetyl chloride → 4-chloro-N'-(2-chloroacetyl)benzohydrazide
Reaktionsgleichung
[Cl:1][C:2]1[CH:11]=[CH:10][C:5]([C:6]([NH:8][NH2:9])=[O:7])=[CH:4][CH:3]=1.[Cl:12][CH2:13][C:14](Cl)=[O:15]>O1CCOCC1>[Cl:12][CH2:13][C:14]([NH:9][NH:8][C:6](=[O:7])[C:5]1[CH:10]=[CH:11][C:2]([Cl:1])=[CH:3][CH:4]=1)=[O:15]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
To a solution of p-chlorobenzoic hydrazide (11.2 g) in dioxane (100 ml) was added chIoroacetyl chloride (6 ml). The resulting mixture was refluxed for three hours, cooled to room temperature and filtered. The resulting solid was washed with ethyl ether and dried to yield N'-chloroacetyl-4-chlorobenzoic hydrazide as white solid.
Aufarbeitung
- temperatureThe resulting mixture was refluxed for three hours
- filtrationfiltered
- washThe resulting solid was washed with ethyl ether
- customdried
Quellen und Nachweise
- ORD-Eintrag
- ord-20add643e25f4ff484bb9c80dc811185
- Quelldatensatz
- uspto-grants-1998_03
- Patentnummer
- US05728694
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