Thionyl Chloride → HCID 58424408, Verbindung
Reaktionsgleichung
[Br:1][C:2]1[CH:14]=[CH:13][C:5]([O:6][CH2:7][CH2:8][CH2:9][C:10](O)=[O:11])=[CH:4][CH:3]=1.O=S(Cl)[Cl:17]>>[Br:1][C:2]1[CH:14]=[CH:13][C:5]([O:6][CH2:7][CH2:8][CH2:9][C:10]([Cl:17])=[O:11])=[CH:4][CH:3]=1Komponenten
3
Versuchsvorschrift
4-(4-Bromophenoxy)butanoic acid (39 g, 25.6 mmol) was dissolved in SOCl2(100 ml) mixture was heated to refluxed overnight. the mixture was concentrated in vacuo to give 4-(4-bromophenoxy)butanoyl chloride (27.6 g, 67%).
Aufarbeitung
- temperaturewas heated
- temperatureto refluxed overnight
- concentrationthe mixture was concentrated in vacuo
Quellen und Nachweise
- ORD-Eintrag
- ord-96dfd8d2418a45dcbca793d91e1166ea
- Quelldatensatz
- uspto-grants-2013_05
- Patentnummer
- US08450308B2
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