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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2100472Erstellt: 26. Oktober 2026

5-(4-Fluoro-phenyl)-4-methyl-pent-4-enoic acid ethyl ester → 5-(4-Fluoro-phenyl)-4-methyl-pentanoic acid ethyl ester

https://huagongshe.com/reaction/2100472

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt5-(4-Fluoro-phenyl)-4-methyl-pent-4-enoic acid ethyl esterHCID 68564929—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthanolHCID 702—
Produkt5-(4-Fluoro-phenyl)-4-methyl-pentanoic acid ethyl esterHCID 68567835—

Reaktionsschritte

A slurry of palladium on charcoal (10%, 1.00 g) and 5-(4-fluoro-phenyl)-4-methyl-pent-4-enoic acid ethyl ester (1.01 g) in ethanol (20 ml) was stirred for 2 h under an atmosphere of hydrogen. The reaction mixture was filtered (dicalite), and the solvent was evaporated. Upon evaporation of the solvent, 5-(4-fluoro-phenyl)-4-methyl-pentanoic acid ethyl ester was obtained; the compound was used in the next step without further purification. MS: m/e=239.3 [M+H+].

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07572801B2
Quelldatensatzuspto-grants-2009_08
ORD IDord-50134e9f42674f89945b28c497940af7
Quellennotizuspto-grants-2009_08