HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-(4-Fluoro-phenyl)-4-methyl-pent-4-enoic acid ethyl ester → 5-(4-Fluoro-phenyl)-4-methyl-pentanoic acid ethyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-(4-Fluoro-phenyl)-4-methyl-pent-4-enoic acid ethyl ester | HCID 68564929 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 5-(4-Fluoro-phenyl)-4-methyl-pentanoic acid ethyl ester | HCID 68567835 | — |
Reaktionsschritte
A slurry of palladium on charcoal (10%, 1.00 g) and 5-(4-fluoro-phenyl)-4-methyl-pent-4-enoic acid ethyl ester (1.01 g) in ethanol (20 ml) was stirred for 2 h under an atmosphere of hydrogen. The reaction mixture was filtered (dicalite), and the solvent was evaporated. Upon evaporation of the solvent, 5-(4-fluoro-phenyl)-4-methyl-pentanoic acid ethyl ester was obtained; the compound was used in the next step without further purification. MS: m/e=239.3 [M+H+].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07572801B2 |
| Quelldatensatz | uspto-grants-2009_08 |
| ORD ID | ord-50134e9f42674f89945b28c497940af7 |
| Quellennotiz | uspto-grants-2009_08 |