HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,1,1-Trifluoro-2,4-pentanedione → HCID 11509542, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,1,1-Trifluoro-2,4-pentanedione | HCID 73943 | — |
| Edukt | (2-Amino-5-trifluoromethoxy-phenyl)-phenyl-methanone | HCID 767339 | — |
| Lösungsmittel | Ethylacetate heptane | HCID 21899848 | — |
| Produkt | HCID 11509542 | HCID 11509542 | 63% |
Reaktionsschritte
The title compound was prepared from (2-Amino-5-trifluoromethoxy-phenyl)-phenyl-methanone [example A6] and 1,1,1-trifluoro-2,4-pentanedione according to the procedure of example 1, except that the reaction time was of 44 h and heptane/ethyl acetate (10:1) was used. Yield: 63%; MS: m/z=399 (M).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07576217B2 |
| Quelldatensatz | uspto-grants-2009_08 |
| ORD ID | ord-665bd1ffe1b9419e9c54b11e6dd3a925 |
| Quellennotiz | uspto-grants-2009_08 |