Thionyl Chloride → HCID 53915754, Verbindung

HRID 2107075Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2107075
[CH:1]([C:3]1([C:12]([OH:14])=O)[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2].S(Cl)([Cl:17])=O>>[CH:1]([C:3]1([C:12]([Cl:17])=[O:14])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2]

Komponenten

3

Edukt 2

HCID 24386Thionyl ChlorideHCID 19828700HCID 19828700, Verbindung

Produkt 1

HCID 53915754HCID 53915754, Verbindung

Versuchsvorschrift

A mixture 2,3-dihydro-2-vinyl-1H-indene-2-carboxylic acid (5.09 g) and thionyl chloride (25 ml) was refluxed for 10 hours. Excess thionyl chloride was distilled off under reduced pressure. The crude product was used as such for the following reaction.

Aufarbeitung

  1. distillationExcess thionyl chloride was distilled off under reduced pressure
  2. customsuch for the following reaction

Quellen und Nachweise

ORD-Eintrag
ord-3181891f19eb44b699d84eb8b2c27787
Quelldatensatz
uspto-grants-1990_06
Patentnummer
US04933359

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