HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate → 2-Allylaminothiazol-4-ylmethanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate | HCID 7171906 | — |
| Edukt | Aluminium lithium hydride | HCID 21226445 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 2-Allylaminothiazol-4-ylmethanol | HCID 15053559 | — |
Reaktionsschritte
The reaction described in Preparation 15 was repeated, but using 10 g of ethyl 2-allylaminothiazole-4-carboxylate, 2.7 g of lithium aluminum hydride and 150 ml of tetrahydrofuran. giving the title compound as pale brown needles.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04933355 |
| Quelldatensatz | uspto-grants-1990_06 |
| ORD ID | ord-96b70246f9234f0a9c9bdb303be4c2c6 |
| Quellennotiz | uspto-grants-1990_06 |