HCID 15053543, Verbindung → HCID 15053561, Verbindung
Reaktionsgleichung
[C:1]1([N:7]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:8]2[S:9][CH:10]=[C:11]([C:13](OCC)=[O:14])[N:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[C:18]1([N:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[C:8]2[S:9][CH:10]=[C:11]([CH2:13][OH:14])[N:12]=2)[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The reaction described in Preparation 15 was repeated, but using 27 g of ethyl 2-diphenylaminothiazole-4-carboxylate, 4.7 g of lithium aluminum hydride and 400 ml of tetrahydrofuran, giving the title compound as pale yellow prisms.