tert-Butyl carbazate → tert-butyl N'-(quinolin-2-yl)methylene-hydrazinecarboxylate

Beteiligte Stoffe

Reaktionsschritte

A solution of 10.70 g 2-quinolinecarboxaldehyde and 9.00 g tert-butyl hydrazinecarboxylate in 200 ml of ethanol is refluxed for 2 h with stirring. Then the solution is evaporated to dryness and the residue is triturated with diisopropylether, separated off and dried at 50° C.

Herkunft & Nachweise