1-Methyl-3-aminopyrazole → HCID 23092978, Verbindung
Reaktionsgleichung
CO[C:3](=[O:12])[C:4]1[CH:9]=[C:8](I)[CH:7]=[C:6]([OH:11])[CH:5]=1.[SH:13][C:14]1[S:15][CH:16]=[N:17][N:18]=1.[NH2:19][C:20]1[CH:24]=[CH:23][N:22]([CH3:25])[N:21]=1>>[OH:11][CH2:6][CH:5]([CH3:4])[O:11][C:6]1[CH:7]=[C:8]([S:13][C:14]2[S:15][CH:16]=[N:17][N:18]=2)[CH:9]=[C:4]([CH:5]=1)[C:3]([NH:19][C:20]1[CH:24]=[CH:23][N:22]([CH3:25])[N:21]=1)=[O:12]Komponenten
4
Versuchsvorschrift
The compound of Production Example 124 was obtained as a colorless amorphous substance using 3-hydroxy-5-iodobenzoic acid methyl ester, 1-tert-dimethylsiloxy-2-hydroxypropane, 2-mercapto-[1,3,4]thiadiazole and 3-amino-1-methyl-1H-pyrazole, by the same method as in Production Example 74 or 82, a corresponding method, or a combination thereof with an ordinary method.
Aufarbeitung
- custom