HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromoisoquinoline → 1-Bromo-2-methylisoquinolinium tetrafluoroborate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromoisoquinoline | HCID 640963 | — |
| Edukt | Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) | HCID 2735153 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 1-Bromo-2-methylisoquinolinium tetrafluoroborate | HCID 20028971 | — |
Reaktionsschritte
The starting material was prepared by reaction of 1-bromoisoquinoline with trimethyloxonium tetrafluoroborate in CH2Cl2 to give 1-bromo-2-methylisoquinolinium tetrafluoroborate, m.p. 162°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04678781 |
| Quelldatensatz | uspto-grants-1987_07 |
| ORD ID | ord-ac0fd97dbf8d414f8bd35fe6df3a2149 |
| Quellennotiz | uspto-grants-1987_07 |