Methane → 1-Disiloxanol, 1,1,3,3,3-pentamethyl-, 1-acetate

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

A mixture containing 14.8 g of 1,1,1,3,3-pentamethyldisiloxane, 10.0 g of allyl acetate (acetic acid allylester) and 0.01 g of palladium supported on activated charcoal, in which the 0.1 g refers to the total weight of the charcoal and the palladium, is heated to boiling under reflux (approximately 105° C.) for 4 hours. The 1,1,1,3,3-pentamethyl-3-acetoxydisiloxane yield is quantitative.

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