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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 21426Erstellt: 25. Oktober 2026

Dichloromethane → 4-Octyl-biphenyl-4'-terephthalic acid chloride

https://huagongshe.com/reaction/21426

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktDichloromethaneHCID 6344—
EduktTerephthaloyl chlorideHCID 7488—
Edukt2-DimethylaminopyridineHCID 21885—
Edukt4'-Octyl-[1,1'-biphenyl]-4-olHCID 14047211—
LösungsmittelTriethylamineHCID 8471—
Produkt4-Octyl-biphenyl-4'-terephthalic acid chlorideHCID 131719017—

Reaktionsschritte

To a solution of 4-hydroxy-4'-octylbiphenyl (0.5 g) and terephthaloyl chloride (0.36 g) in about dichloromethane (30 ml) was added drop by drop triethylamine (0.2 g). To the solution was added dimethylaminopyridine (0.013 g) and the mixture was stirred at the room temperature for 10 hours to obtain the titled compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05424005
Quelldatensatzuspto-grants-1995_06
ORD IDord-2394b2dec9d049a3b2e5b53f9d321778
Quellennotizuspto-grants-1995_06