HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclopentanol → Cyclopentyl 4-methylbenzene-1-sulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclopentanol | HCID 7298 | — |
| Edukt | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | Cyclopentyl 4-methylbenzene-1-sulfonate | HCID 317685 | 68,1% |
Reaktionsschritte
Cyclopentanol (50.0 g, 0.58 mol) and p-toluenesulfonyl chloride (120 g, 0.629 mol) were dissolved in pyridine (200 ml), and the solution was poured into ice-water (about 1 liter), followed by thoroughly stirring. The precipitated solid was filtered and dried to obtain cyclopentyl p-toluenesulfonate as a white solid (94.9 g, 0.390 mol, 68.1% yield).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05424277 |
| Quelldatensatz | uspto-grants-1995_06 |
| ORD ID | ord-7763fe572c454ab3929f14c2186a331a |
| Quellennotiz | uspto-grants-1995_06 |