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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2164453Erstellt: 27. Oktober 2026

2-Chloro-5-(trifluoromethyl)pyridine → 2-Chloro-5-trichloromethylpyridine

https://huagongshe.com/reaction/2164453

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-Chloro-5-(trifluoromethyl)pyridineHCID 92342—
EduktAluminum(III) ChlorideHCID 6451240—
Produkt2-Chloro-5-trichloromethylpyridineHCID 50293—

Reaktionsschritte

To 18.2 g of 2-chloro-5-trifluoromethyl pyridine, 20 g of aluminum chloride was added in 2 hours, and they were reacted under the predetermined reaction conditions as shown in Table 1. After the completion of the reaction, the reaction product was cooled and then introduced into ice water, and the oil layer was separated by liquid separation. The solvent was removed by distillation to obtain 2-chloro-5-trichloromethyl pyridine.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04504665
Quelldatensatzuspto-grants-1985_03
ORD IDord-d59167c8efd6400badb46632f1a2389d
Quellennotizuspto-grants-1985_03