HCID 13281346, Verbindung → HCID 20403339, Verbindung
Reaktionsgleichung
[CH:1]1[C:6]2[C:7]3[CH:16]=[CH:15][CH:14]=[CH:13][C:8]=3[CH2:9][CH2:10][CH2:11][CH2:12][C:5]=2[C:4]([C:17](O)=[O:18])=[CH:3][CH:2]=1>O1CCCC1>[CH:1]1[C:6]2[C:7]3[CH:16]=[CH:15][CH:14]=[CH:13][C:8]=3[CH2:9][CH2:10][CH2:11][CH2:12][C:5]=2[C:4]([CH2:17][OH:18])=[CH:3][CH:2]=1Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The reaction between 5,6,7,8-tetrahydrodibenzo[a,c]cycloocten-4-carboxylic acid (1.7 g, 0.0067 mole) and borane-tetrahydrofuran complex (1.16 g of a 1.05M solution in tetrahydrofuran) in tetrahydrofuran (50 ml) produced 5,6,7,8-tetrahydrodibenzo[a,c]cycloocten-4-methanol as an oil (1.38 g). The IR and nmr spectra were consistent with the proposed structure.
Quellen und Nachweise
- ORD-Eintrag
- ord-7beed09deb5c48dab61a226aaab3ab33
- Quelldatensatz