HCID 54049138, Verbindung → HCID 13316973, Verbindung
Reaktionsgleichung
[Br:1][CH2:2][CH2:3][CH:4]=[CH:5][CH2:6][CH2:7][C:8]1[CH:15]=[CH:14][C:11]([C:12]#[N:13])=[CH:10][CH:9]=1>C(O)C.[Pt]=O>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:15]=[CH:14][C:11]([C:12]#[N:13])=[CH:10][CH:9]=1Komponenten
4
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
A solution of 10.5 g of 4-(6-bromohex-3-enyl)benzonitrile in 200 ml of absolute ethanol was hydrogenated in the presence of 0.25 g of platinum oxide catalyst. Isolation of the product afforded 10.4 g of 4(6-bromohexyl)benzonitrile as a yellow oil which was distilled at 168°-170° C.(0.01 mm) to produce the compound as a colorless oil which solidified upon cooling.
Quellen und Nachweise
- ORD-Eintrag
- ord-9f69ed0f573d4e0ca2c64afe2fc42d9e
- Quelldatensatz
- uspto-grants-1990_07
- Patentnummer
- US04939267
Notizen zur Reaktion
Wird geladen…