1,3-Propanediol, 2-methylene- → 3-Hexadecylaminothiocarbonyloxy-2-methylenepropan-1-ol

Beteiligte Stoffe

Reaktionsschritte

Hexadecyl isothiocyanate (9.65 g) and 2-methylenepropane-1,3-diol) (3.0 g) were heated with pyridine (17 ml) and 4-dimethylaminopyridine (0.8 g) to 104° C. for 6.5 hours. The mixture was evaporated to dryness in vacuo and chromatographed on a Waters PrepLC®/System 500A using a PrepPAK®-500/SILICA cartridge with ether/chloroform/hexane 2:2:9 as eluent.

Herkunft & Nachweise