Bromomethyl acetate → HCID 68485011, Verbindung

Reaktionsgleichung

[CH2:1]([O:5][C:6]1[CH:7]=[C:8]([CH:12]([C:21]([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=[O:22])[CH2:13][NH:14][CH2:15][C:16]([N:18]([CH3:20])[CH3:19])=[O:17])[CH:9]=[CH:10][CH:11]=1)[CH2:2][CH2:3][CH3:4].Br[CH2:29][O:30][C:31](=[O:33])[CH3:32]>>[CH2:1]([O:5][C:6]1[CH:7]=[C:8]([CH:12]([C:21]([O:23][C:24]([CH3:26])([CH3:25])[CH3:27])=[O:22])[CH2:13][NH:14][CH:15]([CH2:29][O:30][C:31](=[O:33])[CH3:32])[C:16]([N:18]([CH3:20])[CH3:19])=[O:17])[CH:9]=[CH:10][CH:11]=1)[CH2:2][CH2:3][CH3:4]

Komponenten

Edukt 2

HCID 68536Bromomethyl acetate

HCID 68487077HCID 68487077, Verbindung

Produkt 1

HCID 68485011HCID 68485011, Verbindung

Versuchsvorschrift

The title compound was prepared from [2-[2-(3-butoxyphenyl)-(tert-butoxycarbonyl)ethylamino]-N,N-dimethylacetamide and acetic acid bromomethyl ester according to Step 1 of Example 3. Colourless oil (38% yield).

Quellen und Nachweise

ORD-Eintrag: ord-b50019a6f5d64f56a7f0d8988505eb8c
Quelldatensatz: uspto-grants-2015_06
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US09051240B2

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