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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2170271Erstellt: 24. Oktober 2026

Piperonal → Bis(3,4-methylenedioxy)chalcone

https://huagongshe.com/de/reaction/2170271

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPiperonalHCID 8438—
EduktSodium HydroxideHCID 14798—
EduktAcetopiperoneHCID 76622—
LösungsmittelEthanolHCID 702—
ProduktBis(3,4-methylenedioxy)chalconeHCID 294346—

Reaktionsschritte

A mixture of piperonal (460 mg) and 3,4-methylenedioxyacetophenone (500 mg) in ethanol (20 ml) was treated with 1M NaOH solution (4 ml), then the mixture was stirred overnight. The pale yellow crystalline solid was filtered off, washed with water then cold aqueous ethanol and dried to give pure bis(3,4-methylenedioxy)chalcone DC-0006B (476 mg, 53%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09051253B2
Quelldatensatzuspto-grants-2015_06
ORD IDord-f07f4bc4c5814b05824736c9efcf4768
Quellennotizuspto-grants-2015_06