HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Iodo-3-methylbenzoic acid → 3-Methyl-2-(1H-pyrazol-1-YL)benzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Iodo-3-methylbenzoic acid | HCID 2759365 | — |
| Edukt | 2-Chloro-5-ethyl-4,6-dimethylpyrimidine | HCID 19846659 | — |
| Edukt | 3-Fluoro-2-iodobenzoic acid | HCID 22320308 | — |
| Produkt | 3-Methyl-2-(1H-pyrazol-1-YL)benzoic acid | HCID 53409761 | — |
Reaktionsschritte
The title compound was prepared in a manner analogous to Intermediate 36 substituting 3-methyl-2-iodobenzoic acid for 3-fluoro-2-iodobenzoic acid. 1H NMR (500 MHz, CDCl3): 7.79 (d, J=7.4 Hz, 2H), 7.48 (d, J=7.5 Hz, 1H), 7.42 (t, J=7.6 Hz, 1H), 6.53 (s, 1H), 2.07 (s, 3H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09062044B2 |
| Quelldatensatz | uspto-grants-2015_06 |
| ORD ID | ord-55f3504069c942ff9f3cc9adadd3edac |
| Quellennotiz | uspto-grants-2015_06 |