HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2175935Erstellt: 26. Oktober 2026
Ethanol → 6-methyl-3-(2H-1,2,3-triazol-2-yl)picolinic acid
https://huagongshe.com/reaction/2175935
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 6-Methyl-3-(2H-1,2,3-triazol-2-yl)picolinonitrile | HCID 68281582 | — |
| Produkt | 6-methyl-3-(2H-1,2,3-triazol-2-yl)picolinic acid | HCID 59363733 | — |
Reaktionsschritte
To a solution of the title compound of Step A (730 mg, 4 mmol) in EtOH (10 mL) was added 4 N NaOH (1 mL, 4 mmol). The mixture was heated at 100° C. for 24 h. The reaction mixture was concentrated in vacuo to a white solid which was used without further purification in subsequent steps.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US09062078B2 |
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| Quelldatensatz | uspto-grants-2015_06 |
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| ORD ID | ord-eb837fd85db84ac6b61acf6793cc84d7 |
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| Quellennotiz | uspto-grants-2015_06 |
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