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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2175935Erstellt: 26. Oktober 2026

Ethanol → 6-methyl-3-(2H-1,2,3-triazol-2-yl)picolinic acid

https://huagongshe.com/reaction/2175935

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthanolHCID 702—
EduktSodium HydroxideHCID 14798—
Edukt6-Methyl-3-(2H-1,2,3-triazol-2-yl)picolinonitrileHCID 68281582—
Produkt6-methyl-3-(2H-1,2,3-triazol-2-yl)picolinic acidHCID 59363733—

Reaktionsbedingungen

Temperatur100 °C

Reaktionsschritte

To a solution of the title compound of Step A (730 mg, 4 mmol) in EtOH (10 mL) was added 4 N NaOH (1 mL, 4 mmol). The mixture was heated at 100° C. for 24 h. The reaction mixture was concentrated in vacuo to a white solid which was used without further purification in subsequent steps.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09062078B2
Quelldatensatzuspto-grants-2015_06
ORD IDord-eb837fd85db84ac6b61acf6793cc84d7
Quellennotizuspto-grants-2015_06