Methyl iodide → Methyl 3-bromo-5-methoxybenzoate
Reaktionsgleichung
[Br:1][C:2]1[CH:3]=[C:4]([CH:9]=[C:10]([OH:12])[CH:11]=1)[C:5]([O:7][CH3:8])=[O:6].[CH3:13]I>>[Br:1][C:2]1[CH:3]=[C:4]([CH:9]=[C:10]([O:12][CH3:13])[CH:11]=1)[C:5]([O:7][CH3:8])=[O:6]Komponenten
3
Versuchsvorschrift
Methyl 3-bromo-5-hydroxybenzoate (O6.032; 2.52 g) was alkylated with methyl iodide and worked up analogously to the conditions of O5.043. 2.5 g of the title compound were obtained.
Quellen und Nachweise
- ORD-Eintrag
- ord-6d021308f0254f99845c3338ea80401d
- Quelldatensatz
- uspto-grants-2012_06
- Patentnummer
- US08198272B2
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