Hydrazine → 4-(Morpholin-4-yl)butan-1-amine

HRID 21787Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 21787
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][NH2:1])[CH2:4][CH2:5][O:6][CH2:7][CH2:8]1

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 220025214-Morpholinylbutylphthalimide

Produkt 1

HCID 2336114-(Morpholin-4-yl)butan-1-amine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-morpholinylbutylphthalimide (231 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Aufarbeitung

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Quellen und Nachweise

ORD-Eintrag
ord-f2a073210bba45ae9b448c979d5547fb
Quelldatensatz
uspto-grants-1995_06
Patentnummer
US05424451

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