Hydrazine → 6-Morpholin-4-ylhexylamine
Reaktionsgleichung
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][NH2:1])[CH2:4][CH2:5][O:6][CH2:7][CH2:8]1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 6-morpholinylhexylphthalimide (253 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.
Aufarbeitung
- temperaturethe resulting solution was refluxed
- customReaction times and process as per Example 1
Quellen und Nachweise
- ORD-Eintrag
- ord-e59c2a63409148faa6c51aaa64a0397f
- Quelldatensatz
- uspto-grants-1995_06
- Patentnummer
- US05424451
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