Hydrazine → 8-Morpholinooctylamine

HRID 21799Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 21799
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH2:1])[CH2:4][CH2:5][O:6][CH2:7][CH2:8]1

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 537680558-Morpholinyloctylphthalimide

Produkt 1

HCID 222376608-Morpholinooctylamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-morpholinyloctylphthalimide (275 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Aufarbeitung

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Quellen und Nachweise

ORD-Eintrag
ord-6e7e1bb58d654f78818c1c604ca73fed
Quelldatensatz
uspto-grants-1995_06
Patentnummer
US05424451

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