Hydrazine → HCID 54275604, Verbindung

HRID 21807Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 21807
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13][NH2:1]

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 538263884-(N-methylpiperazinyl)butylphthalimide

Produkt 1

HCID 54275604HCID 54275604, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-(N-methylpiperazinyl)butylphthalimide (240 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Aufarbeitung

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Quellen und Nachweise

ORD-Eintrag
ord-c944c58f544d4256941c6aa331ac25a9
Quelldatensatz
uspto-grants-1995_06
Patentnummer
US05424451

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