Hydrazine → 8-Piperidinyloctylamine

HRID 21814Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 21814
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]1

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 540305088-Piperidinyloctylphthalimide

Produkt 1

HCID 110092698-Piperidinyloctylamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-piperidinyloctylphthalimide (274 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Aufarbeitung

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Quellen und Nachweise

ORD-Eintrag
ord-e06d024b9acb4c0eadbd0144dfda4742
Quelldatensatz
uspto-grants-1995_06
Patentnummer
US05424451

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