HCID 18782313, Verbindung → HCID 22458144, Verbindung
Reaktionsgleichung
[C:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]([C:27]([CH:29]1[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]1)=[O:28])[CH2:10][CH2:11][N:12]1[CH2:17][CH2:16][N:15]([C:18]2[CH:23]=[CH:22][C:21]([NH2:24])=[CH:20][C:19]=2[O:25][CH3:26])[CH2:14][CH2:13]1)#[N:2].NC1C=CC=CC=1N(C(C1CCCCC1)=O)CCN1CCN([C:51]2C=CC=C[C:52]=2[O:57]C)CC1>>[C:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]([C:27]([CH:29]1[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]1)=[O:28])[CH2:10][CH2:11][N:12]1[CH2:13][CH2:14][N:15]([C:18]2[CH:23]=[CH:22][C:21]([NH:24][C:52](=[O:57])[CH3:51])=[CH:20][C:19]=2[O:25][CH3:26])[CH2:16][CH2:17]1)#[N:2]Komponenten
3
Reaktionsbedingungen
- Temperatur
- 22.5 °C
Versuchsvorschrift
The title compound was synthesized according to the procedure reported in example 28 but substituting the compound of example 79 for the compound of example 27 and stirring at 20-25° C. for 17 h. The usual work-up afforded the title compound. Yield: 49%.
Aufarbeitung
- customThe title compound was synthesized