HCID 22452278, Verbindung → HCID 53733051, Verbindung
Reaktionsgleichung
[CH2:1]([O:3][C:4]([C:6]1[C:7](=[O:20])[NH:8][N:9]=[C:10]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)[CH:11]=1)=[O:5])[CH3:2].[F:21][C:22]1[CH:31]=[C:30]([F:32])[CH:29]=[CH:28][C:23]=1[CH:24]=[CH:25][CH2:26]Cl>>[F:21][C:22]1[CH:31]=[C:30]([F:32])[CH:29]=[CH:28][C:23]=1[CH:24]=[CH:25][CH2:26][N:8]1[C:7](=[O:20])[C:6]([C:4]([O:3][CH2:1][CH3:2])=[O:5])=[CH:11][C:10]([C:12]2[CH:13]=[CH:14][C:15]([O:18][CH3:19])=[CH:16][CH:17]=2)=[N:9]1Komponenten
3
Versuchsvorschrift
Using 4-ethoxycarbonyl-6-(4-methoxyphenyl)-2H-pyridazin-3-one and 2,4-difluorocinnamyl chloride as starting materials, the procedures of Example 1 were repeated likewise, whereby the title compound was obtained in a yield of 92.0%.
Quellen und Nachweise
- ORD-Eintrag
- ord-128fd27d158a4ebe8b68d626d5c515e2
- Quelldatensatz
- uspto-grants-2002_06