HCID 597528, Verbindung → HCID 21349890, Verbindung
Reaktionsgleichung
O[CH2:2][CH2:3][N:4]1[C:9]2[CH:10]=[CH:11][CH:12]=[C:13]([O:14][CH2:15][C:16]([O:18][CH3:19])=[O:17])[C:8]=2[O:7][CH2:6][C:5]1=[O:20].[C:21]1([C:27]([C:30]2[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=2)([SH:29])[CH3:28])[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[C:30]1([C:27]([C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=2)([S:29][CH2:2][CH2:3][N:4]2[C:9]3[CH:10]=[CH:11][CH:12]=[C:13]([O:14][CH2:15][C:16]([O:18][CH3:19])=[O:17])[C:8]=3[O:7][CH2:6][C:5]2=[O:20])[CH3:28])[CH:31]=[CH:32][CH:33]=[CH:34][CH:35]=1Komponenten
3
Versuchsvorschrift
The same process as Example 1 was repeated except that methyl (4-(2-hydroxyethyl)-3-oxo-3,4-dihydro-2H-1,4-benzoxazin-8-yloxy)acetate (187 mg) and 1,1-diphenylethanethiol (270 ml) were used to obtain the object compound (172.5 mg, yield 42%).
Quellen und Nachweise
- ORD-Eintrag
- ord-917b0c011c764d28949bf971607260f2
- Quelldatensatz
- uspto-grants-2002_06