N-benzylaminosulfonamide → Benzylsulfamide potassium salt

HRID 2189129Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2189129
[CH2:1]([NH:8][S:9]([NH2:12])(=[O:11])=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.CC([O-])(C)C.[K+:18]>>[K+:18].[CH2:1]([NH:8][S:9]([NH-:12])(=[O:11])=[O:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Komponenten

3

Edukt 2

HCID 12354987N-benzylaminosulfonamideHCID 23665647Potassium tert-butoxide

Produkt 1

HCID 21041359Benzylsulfamide potassium saltAusbeute 100,6 %

Versuchsvorschrift

To a solution of benzylsulfamide (17.98 g) in McOH (300 mL) was carefully added potassium tert-butylate (10.8 g). The mixture was stirred at rt for 15 min before the solvent was evaporated. The remaining residue was dried under HV to give benzylsulfamide potassium salt as an off-white powder (21.73 g).

Aufarbeitung

  1. customwas evaporated
  2. customThe remaining residue was dried under HV

Quellen und Nachweise

ORD-Eintrag
ord-5d1afc6e2d174f638edd86682471e518
Quelldatensatz
uspto-grants-2012_12
Patentnummer
US08324232B2

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