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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2191851Erstellt: 27. Oktober 2026

Trifluoroacetic acid → 2-((4-(Acetamido)phenyl)amino)-4-phenethylbenzoic acid

https://huagongshe.com/reaction/2191851

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTrifluoroacetic acidHCID 6422—
EduktTert-butyl 2-((4-(acetamido)phenyl)amino)-4-phenethylbenzoateHCID 68957261—
Produkt2-((4-(Acetamido)phenyl)amino)-4-phenethylbenzoic acidHCID 57668063—

Reaktionsschritte

Trifluoroacetic acid 7.5 mL was added to the obtained tert-butyl 2-((4-(acetamido)phenyl)amino)-4-phenethylbenzoate, and it was stirred at room temperature for 2 hours. The solvent was removed under reduced pressure, methanol was added to the obtained residue, and solid matter was filtrated to give 2-((4-(acetamido)phenyl)amino)-4-phenethylbenzoic acid 23 mg of a white solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08327467B2
Quelldatensatzuspto-grants-2012_12
ORD IDord-b9853af598904e009feca33baf0fa0b5
Quellennotizuspto-grants-2012_12