2-Bromoethyl methyl ether → 4-[2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl]-1-(2-methoxy-ethyl)-1H-pyridin-2-one
Reaktionsgleichung
[CH3:1][C:2]1[N:3]([C:17]2[CH:22]=[CH:21][NH:20][C:19](=[O:23])[CH:18]=2)[C:4]([CH3:16])=[C:5]([C:7]#[C:8][C:9]2[CH:10]=[C:11]([CH3:15])[CH:12]=[CH:13][CH:14]=2)[N:6]=1.Br[CH2:25][CH2:26][O:27][CH3:28]>>[CH3:1][C:2]1[N:3]([C:17]2[CH:22]=[CH:21][N:20]([CH2:25][CH2:26][O:27][CH3:28])[C:19](=[O:23])[CH:18]=2)[C:4]([CH3:16])=[C:5]([C:7]#[C:8][C:9]2[CH:10]=[C:11]([CH3:15])[CH:12]=[CH:13][CH:14]=2)[N:6]=1Komponenten
3
Versuchsvorschrift
The title compound, light brown solid, MS: m/e=362.3 (M+H+), was prepared in accordance with the general method of example 3 from 4-[2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl]-1H-pyridin-2-one and 2-bromoethyl-methylether.
Quellen und Nachweise
- ORD-Eintrag
- ord-e385306d75514e0cbdfdca68b17737f5
- Quelldatensatz
- uspto-grants-2012_12