HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Salicyl Alcohol → 2-[(Ethylsulfanyl)methyl]phenol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Salicyl Alcohol | HCID 5146 | — |
| Edukt | Ethanethiol | HCID 6343 | — |
| Produkt | 2-[(Ethylsulfanyl)methyl]phenol | HCID 522167 | 96% |
Reaktionsschritte
A mixture of 49.6 g (0.4 mol) of 2-hydroxymethyl-phenol and 124 g (2 mol) of ethylmercaptan was heated for 5 hours to 170° C. in a stirred autoclave. Working up as in Example 1 gave 32.2 g (96% of theory) of 2-ethylthiomethyl-phenol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04358616 |
| Quelldatensatz | uspto-grants-1982_11 |
| ORD ID | ord-eacb17e009e84059b307f1326fc1641a |
| Quellennotiz | uspto-grants-1982_11 |