HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Anhydride → N-(4-Fluoro-2-methylphenyl)acetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Anhydride | HCID 7918 | — |
| Edukt | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| Produkt | N-(4-Fluoro-2-methylphenyl)acetamide | HCID 2737623 | 74% |
Reaktionsschritte
A mixture of 4-fluoro-2-methylaniline (20 g) and (CH3CO)2O (400 mL) was stirred at RT for 3 hours. The reaction mixture was subsequently poured into ice water (1000 mL), stirred for 10 minutes, filtered, and dried under vacuum to give the title compound (20 g, 74%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09365566B2 |
| Quelldatensatz | uspto-grants-2016_06 |
| ORD ID | ord-259c4edab98645ea991b35ce6b268676 |
| Quellennotiz | uspto-grants-2016_06 |