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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2205252Erstellt: 26. Oktober 2026

1,2-Dichloroethane → 1-(2-(2,3-Dimethylbut-2-en-1-yl)indolin-1-yl)ethanone

https://huagongshe.com/reaction/2205252

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1,2-DichloroethaneHCID 11—
EduktIndoleHCID 798—
EduktTin tetrachlorideHCID 24287—
Edukt3H-IndoleHCID 3083560—
Edukt3,3,4-Trimethylpent-4-en-2-oneHCID 13262537—
Produkt1-(2-(2,3-Dimethylbut-2-en-1-yl)indolin-1-yl)ethanoneHCID 7152587958%

Reaktionsschritte

Following the general procedure as described in Example 11, 3,3,4-trimethylpent-4-en-2-one (0.50 g, 3.96 mmol), 1H-indole (0.56 g, 4.75 mmol) which was in situ isomerized to 3H-indole, and SnCl4 (1.24 g, 4.75 mmol) in 1,2-dichloroethane (40 ml) were reacted to give the title product as a white solid (0.56 g, 58%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09371262B2
Quelldatensatzuspto-grants-2016_06
ORD IDord-cfeb19e361a74c21b17c8dd50fedbe70
Quellennotizuspto-grants-2016_06