HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Trichloro(chloromethyl)silane → Chloromethyldichloro(4-fluorophenyl)silane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Trichloro(chloromethyl)silane | HCID 15258 | — |
| Edukt | HCID 178418676 | HCID 178418676 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | Chloromethyldichloro(4-fluorophenyl)silane | HCID 19382008 | — |
Reaktionsschritte
In the same apparatus as Example 1, was added 5.6 g of chloromethyltrichlorosilane (0.03 mol) and 50 ml of THF. Through the dropping funnel was firstly added 22 ml of 4-fluorophenylmagnesiumbromide (2.0 M in diethylether) to give chloromethyldichloro(4-fluorophenyl)silane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05455356 |
| Quelldatensatz | uspto-grants-1995_10 |
| ORD ID | ord-9a42c4cfd268423fa50241803e4fe507 |
| Quellennotiz | uspto-grants-1995_10 |