N-(oxan-4-ylidene)hydroxylamine → tetrahydropyran-4-one O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio]-alpha-methylbenzyl}oxime

Beteiligte Stoffe

Reaktionsschritte

Using an analogous procedure to that described in Example 1, tetrahydropyran-4-one oxime was reacted with 4-{3-[4-(1-chloroethyl)-phenylthio] -5-fluorophenyl}-4-methoxytetrahydropyran to give tetrahydropyran-4-one O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)-phenylthio]-α-methylbenzyl}oxime as an oil in 74% yield.

Herkunft & Nachweise