N-(4-hydroxy-2,3,6-trimethylphenyl)formamide → N-[4-[[(E)-3-(4-Isopropylphenyl)-2-propenyl]oxy]-2,3,6-trimethylphenyl]formamide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	N-(4-hydroxy-2,3,6-trimethylphenyl)formamide	HCID 21961295	—
Edukt	1-[(E)-3-bromo-1-propenyl]-4-isopropylbenzene	HCID 21961313	—
Lösungsmittel	Ethyl acetate hexane	HCID 21226206	—
Produkt	N-[4-[[(E)-3-(4-Isopropylphenyl)-2-propenyl]oxy]-2,3,6-trimethylphenyl]formamide	HCID 21961342	59%

Reaktionsschritte

By using N-(4-hydroxy-2,3,6-trimethylphenyl)formamide and 1-[(E)-3-bromo-1-propenyl]-4-isopropylbenzene, the title compound was synthesized according to Reference Example 17a. Yield: 59%. Melting point: 165-167° C. (Ethyl acetate-hexane).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US07101867B2
Quelldatensatz	uspto-grants-2006_09
ORD ID	ord-495416fcdabc447c842a415e4c44d07f
Quellennotiz	uspto-grants-2006_09