Benzyl chloromethyl ether → tert-Butyl 4-[(Benzyloxy)methyl]hexahydro-3-oxo-1H-1,4-diazepine-1-carboxylate

HRID 2211847

Reaktionsgleichung

Reaktionsgleichung von HRID 2211847
[O:1]=[C:2]1[NH:8][CH2:7][CH2:6][CH2:5][N:4]([C:9]([O:11][C:12]([CH3:15])([CH3:14])[CH3:13])=[O:10])[CH2:3]1.Cl[CH2:17][O:18][CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[CH2:19]([O:18][CH2:17][N:8]1[CH2:7][CH2:6][CH2:5][N:4]([C:9]([O:11][C:12]([CH3:15])([CH3:14])[CH3:13])=[O:10])[CH2:3][C:2]1=[O:1])[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1

Komponenten

3

Edukt 2

HCID 137983Benzyl chloromethyl etherHCID 21962087tert-Butyl 3-oxo-1,4-diazepane-1-carboxylate

Produkt 1

HCID 21962085tert-Butyl 4-[(Benzyloxy)methyl]hexahydro-3-oxo-1H-1,4-diazepine-1-carboxylate

Versuchsvorschrift

The title compound was prepared from tert-butyl hexahydro-3-oxo-1H-1,4-diazepine-1-carboxylate (Example 2, Step B) and benzyl chloromethyl ether essentially following the method described in Example 2, Step C.

Quellen und Nachweise

ORD-Eintrag
ord-3f096680a3d546ada0649f4e2c7ef0cd
Quelldatensatz
uspto-grants-2006_09
Patentnummer
US07101871B2

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