HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Acetylpyridine → 4-(2,4-Dioxo-4-pyridin-4-ylbutoxy)piperidine-1-carboxylic acid tert-butyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Acetylpyridine | HCID 14282 | — |
| Edukt | 2-((1-((Tert-butoxy)carbonyl)piperidin-4-yl)oxy)acetic acid | HCID 1502082 | — |
| Produkt | 4-(2,4-Dioxo-4-pyridin-4-ylbutoxy)piperidine-1-carboxylic acid tert-butyl ester | HCID 57954445 | — |
Reaktionsschritte
Condensation of 4-acetylpyridine with 4-carboxymethoxypiperidine-1-carboxylic acid tert-butyl ester (Preparation 1), employing the protocol described in Preparation 22, afforded the title compound: m/z (ES+)=263.2 [M-Boc+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08207147B2 |
| Quelldatensatz | uspto-grants-2012_06 |
| ORD ID | ord-4722c3c8e618440fbf5e176229b823ec |
| Quellennotiz | uspto-grants-2012_06 |