4-(Dimethylamino)Benzaldehyde → [(4-Dimethylaminophenyl)methyl](4-ethylphenyl)amine

HRID 2213585

Reaktionsgleichung

[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH2:12]([C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[CH:16][CH:15]=1)[CH3:13]>>[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:18][C:17]2[CH:19]=[CH:20][C:14]([CH2:12][CH3:13])=[CH:15][CH:16]=2)=[CH:5][CH:4]=1

Komponenten

Edukt 2

HCID 74794-(Dimethylamino)Benzaldehyde

HCID 115044-Ethylaniline

Produkt 1

HCID 3482181[(4-Dimethylaminophenyl)methyl](4-ethylphenyl)amineAusbeute 62,8 %

Versuchsvorschrift

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (10 g) and 4-ethylaniline (8.12 g) as starting materials, [(4-dimethylaminophenyl)methyl](4-ethylphenyl)amine (10.7 g) was obtained. melting point: 64–66° C.

Aufarbeitung

customBy the reaction and treatment in the same manner

Quellen und Nachweise

ORD-Eintrag: ord-109b14d068bf435b9db2073fdb5eff4b
Quelldatensatz: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07105567B2

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