HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzonitrile → 1-Phenyl-1-hexyne
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzonitrile | HCID 7505 | — |
| Edukt | Phenylacetylene | HCID 10821 | — |
| Edukt | 1-Hexyne | HCID 12732 | — |
| Produkt | 1-Phenyl-1-hexyne | HCID 136908 | 95% |
Reaktionsschritte
The procedure was identical to Example 1, with the exception that 1-hexyne (0.450 ml; 0.329 g; 4.00 mmol) was used as a substrate instead of phenylacetylene. GC analysis of the organic phase of the hydrolyzed reaction sample after 20 h at 65° C. showed the presence of 1.90 mmol (95% yield) of 1-hexynylbenzene and and 0.08 mmol of benzonitrile remaining in the reaction mixture.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07105707B2 |
| Quelldatensatz | uspto-grants-2006_09 |
| ORD ID | ord-585442bfbe2140c0afdecb052599d445 |
| Quellennotiz | uspto-grants-2006_09 |